2X0K
Crystal structure of modular FAD synthetase from Corynebacterium ammoniagenes
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 3 |
Unit cell lengths | 133.472, 133.472, 133.472 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 94.490 - 1.950 |
R-factor | 0.20676 |
Rwork | 0.204 |
R-free | 0.23711 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.993 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.230 | 2.060 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.090 | 0.460 |
Number of reflections | 57834 | |
<I/σ(I)> | 19.9 | 2.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.4 | 8.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 1.5M LI2SO4, 0.1 M HEPES-NAOH, PH 7.5 | ||
1 | 7.5 | 1.5M LI2SO4, 0.1 M HEPES-NAOH, PH 7.5 |