2WZZ
AMP-C BETA-LACTAMASE (PSEUDOMONAS AERUGINOSA)IN COMPLEX WITH compound M-03
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2006-07-14 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.791, 72.575, 106.271 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.930 - 1.570 |
R-factor | 0.18139 |
Rwork | 0.181 |
R-free | 0.19659 |
Structure solution method | OTHER |
RMSD bond length | 0.008 |
RMSD bond angle | 1.206 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.570 |
Rmerge | 0.100 |
Number of reflections | 48596 |
<I/σ(I)> | 20.3 |
Completeness [%] | 100.0 |
Redundancy | 8.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |