2WZO
The structure of the FYR domain
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 53.867, 53.867, 91.297 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 23.325 - 1.600 |
R-factor | 0.1793 |
Rwork | 0.178 |
R-free | 0.20190 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.391 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.600 | |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.080 | 0.420 |
Number of reflections | 20876 | |
<I/σ(I)> | 18.8 | 5.7 |
Completeness [%] | 99.8 | 98.9 |
Redundancy | 10.4 | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 1.0M POTASSIUM/SODIUM TARTRATE, 100MM HEPES, PH7.5, AT 17OC. 20% GLYCEROL USED AS A CRYOPROTECTANT. |