2WZ9
Crystal structure of the thioredoxin domain of human TXNL2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-09-25 |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 42.630, 52.060, 58.600 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 58.600 - 1.550 |
| R-factor | 0.156 |
| Rwork | 0.154 |
| R-free | 0.17900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2diy |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.578 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0089) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.470 | 1.630 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Rmerge | 0.090 | 0.580 |
| Number of reflections | 19534 | |
| <I/σ(I)> | 9.5 | 2.2 |
| Completeness [%] | 99.8 | 99.6 |
| Redundancy | 3.8 | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 1.4 M AMMONIUM CITRATE, PH 7 |
