2WZ8
Family 35 carbohydrate binding module from Clostridium thermocellum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.814, 52.914, 58.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.270 - 1.500 |
R-factor | 0.1326 |
Rwork | 0.130 |
R-free | 0.17538 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2w1w |
RMSD bond length | 0.015 |
RMSD bond angle | 1.457 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MrBUMP |
Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.050 | 0.120 |
Number of reflections | 20322 | |
<I/σ(I)> | 37.3 | 12.1 |
Completeness [%] | 97.1 | 95.8 |
Redundancy | 6.9 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2 M MAGNESIUM ACETATE, 30% PEG 3350 |