2WYT
1.0 A resolution structure of L38V SOD1 mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX10.1 |
Synchrotron site | SRS |
Beamline | PX10.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-12 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.690, 67.345, 52.577 |
Unit cell angles | 90.00, 106.57, 90.00 |
Refinement procedure
Resolution | 24.000 - 1.000 |
R-factor | 0.12501 |
Rwork | 0.124 |
R-free | 0.14677 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2c9v |
RMSD bond length | 0.018 |
RMSD bond angle | 1.838 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0106) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.000 | 1.020 |
High resolution limit [Å] | 1.000 | 1.000 |
Rmerge | 0.120 | 0.360 |
Number of reflections | 136867 | |
<I/σ(I)> | 14 | 2.2 |
Completeness [%] | 98.3 | 77.3 |
Redundancy | 5.4 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.75 | 150 MM NACL, 2-3M AMMONIUM SULPHATE, 100 MM NA ACETATE BUFFER PH 4.75 |