2WWS
Physalis Mottle Virus: Natural Empty Capsid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 300 |
Detector technology | IMAGE PLATE |
Collection date | 2004-09-18 |
Detector | MARRESEARCH |
Spacegroup name | H 3 |
Unit cell lengths | 325.760, 325.760, 738.940 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 3.900 |
R-factor | 0.2299 |
Rwork | 0.230 |
R-free | 0.24250 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.532 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.000 | 4.040 |
High resolution limit [Å] | 3.900 | 3.900 |
Rmerge | 0.130 | |
Number of reflections | 266460 | |
<I/σ(I)> | 8 | |
Completeness [%] | 87.9 | 89.1 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 100MM SODIUM ACETATE, 2MM CALCL2, 10% GLYCEROL, 3% PEG8000 PH 5.5. |