2WW7
foldon containing beta-turn mimic
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-02-02 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 |
| Unit cell lengths | 27.730, 28.500, 48.755 |
| Unit cell angles | 77.25, 88.00, 69.45 |
Refinement procedure
| Resolution | 26.020 - 1.060 |
| R-factor | 0.10832 |
| Rwork | 0.108 |
| R-free | 0.14024 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1nay |
| RMSD bond length | 0.010 |
| RMSD bond angle | 2.809 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 1.120 |
| High resolution limit [Å] | 1.060 | 1.060 |
| Rmerge | 0.030 | 0.070 |
| Number of reflections | 58056 | |
| <I/σ(I)> | 19.2 | 9.5 |
| Completeness [%] | 94.1 | 86.8 |
| Redundancy | 2 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 9 MM POTASSIUM PHOSPHATE, PH 7.0, 10% D2O |
