2WW6
foldon containing D-amino acids in turn positions
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-02-02 |
| Detector | ADSC CCD |
| Spacegroup name | P 32 |
| Unit cell lengths | 29.830, 29.830, 75.080 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 17.980 - 0.980 |
| R-factor | 0.12979 |
| Rwork | 0.129 |
| R-free | 0.14710 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1nay |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.246 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.030 |
| High resolution limit [Å] | 0.980 | 0.980 |
| Rmerge | 0.050 | 0.280 |
| Number of reflections | 42623 | |
| <I/σ(I)> | 10.4 | 2.8 |
| Completeness [%] | 99.2 | 98.4 |
| Redundancy | 2.3 | 2.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 9 MM POTASSIUM PHOSPHATE, PH 7.0, 10% D2O |
