2WW4
a triclinic crystal form of E. coli 4-diphosphocytidyl-2C-methyl-D- erythritol kinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 49.051, 50.124, 66.035 |
Unit cell angles | 88.77, 69.65, 65.14 |
Refinement procedure
Resolution | 24.890 - 2.000 |
R-factor | 0.20047 |
Rwork | 0.197 |
R-free | 0.26224 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oj4 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.328 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0094) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.900 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.060 | 0.190 |
Number of reflections | 31885 | |
<I/σ(I)> | 5.6 | 2.9 |
Completeness [%] | 94.0 | 93.3 |
Redundancy | 1.9 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |