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2WUY

the crystal structure of wild-type baculovirus polyhedra

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyCCD
Collection date2009-07-13
DetectorMARRESEARCH
Spacegroup nameI 2 3
Unit cell lengths101.562, 101.562, 101.562
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution41.460 - 3.090
R-factor0.206
Rwork0.205
R-free0.23780
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2wux
RMSD bond length0.007
RMSD bond angle0.940
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareBUSTER (2.9.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0003.110
High resolution limit [Å]3.0003.000
Rmerge0.380
Number of reflections3329
<I/σ(I)>4.41.4
Completeness [%]99.6100
Redundancy6.86.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
17.5pH 7.5

247536

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