2WUI
Crystal Structure of MexZ, a key repressor responsible for antibiotic resistance in Pseudomonas aeruginosa.
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 287 |
Detector technology | CCD |
Detector | ADSC CCD |
Wavelength(s) | 1.0000, 0.9791, 0.9793, 0.9757 |
Spacegroup name | H 3 2 |
Unit cell lengths | 177.055, 177.055, 54.658 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.384 - 2.900 |
R-factor | 0.2291 |
Rwork | 0.227 |
R-free | 0.27680 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.729 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 88.500 |
High resolution limit [Å] | 2.900 |
Rmerge | 0.080 |
Number of reflections | 7354 |
<I/σ(I)> | 6.6 |
Completeness [%] | 99.5 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |