2WTP
Crystal Structure of Cu-form Czce from C. metallidurans CH34
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 105.000, 29.530, 71.170 |
Unit cell angles | 90.00, 113.41, 90.00 |
Refinement procedure
Resolution | 19.141 - 1.500 |
R-factor | 0.1613 |
Rwork | 0.160 |
R-free | 0.18850 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.026 |
RMSD bond angle | 2.448 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.140 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.040 | 0.240 |
Number of reflections | 32477 | |
<I/σ(I)> | 17.6 | 5.5 |
Completeness [%] | 99.4 | 97.9 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | PEG4K, MGCL2, TRIS PH 8.5, GLYCEROL |