2WS2
The 2 Angstrom structure of a Nu-class GST from Haemonchus contortus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-03-29 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.216, 101.382, 47.170 |
Unit cell angles | 90.00, 100.46, 90.00 |
Refinement procedure
Resolution | 50.710 - 2.010 |
R-factor | 0.23591 |
Rwork | 0.233 |
R-free | 0.28983 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1tw9 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.891 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 14.000 | 2.030 |
High resolution limit [Å] | 2.010 | 2.000 |
Rmerge | 0.120 | 0.510 |
Number of reflections | 28361 | |
<I/σ(I)> | 124.39 | 2.44 |
Completeness [%] | 97.7 | 97.2 |
Redundancy | 4.69 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 100MM TRIS HCL, PH 8.5, 50 MM CACL2, 30% (W/V) PEG 10000 |