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2WRW

Semi-synthetic highly active analogue of human insulin D-ProB26-DTI- NH2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]100
Detector technologyCCD
Collection date2009-02-19
DetectorADSC CCD
Spacegroup nameI 41 2 2
Unit cell lengths39.372, 39.372, 123.928
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution25.000 - 2.410
R-factor0.23931
Rwork0.237
R-free0.30086
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1mso
RMSD bond length0.017
RMSD bond angle1.632
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.5.0088)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.450
High resolution limit [Å]2.4102.410
Rmerge0.0600.220
Number of reflections2438
<I/σ(I)>14.69.2
Completeness [%]98.598.1
Redundancy65
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
130.015 M CS2SO4 PH 3.0

225158

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