2WQA
Complex of TTR and RBP4 and Oleic Acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2007-10-14 |
Detector | ADSC CCD |
Spacegroup name | P 41 |
Unit cell lengths | 138.662, 138.662, 122.789 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 92.060 - 2.850 |
R-factor | 0.2279 |
Rwork | 0.227 |
R-free | 0.25319 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jyd |
RMSD bond length | 0.015 |
RMSD bond angle | 1.562 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.990 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.060 | 0.670 |
Number of reflections | 54072 | |
<I/σ(I)> | 21.97 | 2.95 |
Completeness [%] | 99.5 | 99.5 |
Redundancy | 7.5 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |