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2WQ3

GCN4 leucine zipper mutant with three IxxNTxx motifs coordinating chloride and nitrate

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyCCD
DetectorMARRESEARCH
Spacegroup nameI 21 3
Unit cell lengths56.670, 56.670, 56.670
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution23.140 - 1.220
R-factor0.14351
Rwork0.141
R-free0.19989
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2wq1
RMSD bond length0.019
RMSD bond angle1.510
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareMOLREP
Refinement softwareREFMAC (5.5.0072)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]23.0001.300
High resolution limit [Å]1.2201.220
Rmerge0.0400.630
Number of reflections9094
<I/σ(I)>17.62.01
Completeness [%]99.499.5
Redundancy3.573.49
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
125,5% (W/V) PEG 4000, 15% (V/V) GLYCEROL, 170MM NA-ACETATE, 90MM TRIS PH 8.5

217705

PDB entries from 2024-03-27

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