2WOR
co-structure of S100A7 with 1,8 ANS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-17 |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 51.660, 51.660, 117.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.270 - 1.700 |
R-factor | 0.188 |
Rwork | 0.187 |
R-free | 0.21211 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2psr |
RMSD bond length | 0.033 |
RMSD bond angle | 2.563 |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.210 | 1.740 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.070 | 0.350 |
Number of reflections | 18214 | |
<I/σ(I)> | 34.1 | 9.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 26.4 | 22.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |