2WOH

Strontium soaked E. coli copper amine oxidase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	RIGAKU IMAGE PLATE
Spacegroup name	P 21 21 21
Unit cell lengths	135.135, 166.911, 79.796
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.820 - 2.700
R-factor	0.18847
Rwork	0.186
R-free	0.24280
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.004
RMSD bond angle	0.853
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.5.0066)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.600	2.850
High resolution limit [Å]	2.700	2.700
Rmerge	0.070	0.300
Number of reflections	49169
<I/σ(I)>	14.3	3.6
Completeness [%]	98.1	99.5
Redundancy	3.1	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1