2WNK
Structure of SporoSAG from Toxoplasma gondii
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Collection date | 2008-06-06 |
| Detector | RIGAKU |
| Spacegroup name | P 6 |
| Unit cell lengths | 106.496, 106.496, 31.616 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 23.420 - 1.550 |
| R-factor | 0.20395 |
| Rwork | 0.202 |
| R-free | 0.24589 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.957 |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | autoSHARP |
| Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.700 | 1.590 |
| High resolution limit [Å] | 1.500 | 1.550 |
| Rmerge | 0.040 | 0.480 |
| Number of reflections | 30054 | |
| <I/σ(I)> | 19.9 | 52.6 |
| Completeness [%] | 99.3 | 99.7 |
| Redundancy | 4.3 | 4.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
