2WLB
Adrenodoxin-like ferredoxin Etp1fd(516-618) of Schizosaccharomyces pombe mitochondria
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU H2B |
Temperature [K] | 278 |
Detector technology | IMAGE PLATE |
Collection date | 2004-04-06 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 81.965, 81.965, 68.289 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.600 |
R-factor | 0.184 |
Rwork | 0.182 |
R-free | 0.23500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 1E6E 1ayf 1l6v 2bt6 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.453 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SWISS-MODELLER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.780 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.110 | 0.510 |
Number of reflections | 8006 | |
<I/σ(I)> | 8.5 | 3.4 |
Completeness [%] | 99.5 | 92.4 |
Redundancy | 3.4 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 277 | VAPOUR DIFFUSION, SITTING DROP, 4 DEGR. CENTIGRADE. RESERVOIR: 0.04M HEPES,1.8M NA-CITRATE, 3% GLYCEROL,PH7.0. PROTEIN SOLUTION: 18.4MG/ML PROTEIN, 20MM POTASSIUMPHOSPHATE,PH7.4. 0.3 PLUS 0.3 MICROLITER DROPLET. |