2WKK
Identification of the glycan target of the nematotoxic fungal galectin CGL2 in Caenorhabditis elegans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-28 |
Detector | RAYONIX |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.210, 80.620, 120.630 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.295 - 1.500 |
R-factor | 0.1511 |
Rwork | 0.150 |
R-free | 0.18590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ulg |
RMSD bond length | 0.009 |
RMSD bond angle | 1.685 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.300 | 1.600 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.070 | 0.790 |
Number of reflections | 17766 | |
<I/σ(I)> | 23.08 | 2.74 |
Completeness [%] | 99.7 | 98.3 |
Redundancy | 12.68 | 8.17 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |