2WKA
Structure of Plp_Thr_decanoyl-CoA aldimine form of Vibrio cholerae CqsA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 178.030, 70.570, 70.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.810 - 1.910 |
R-factor | 0.203 |
Rwork | 0.200 |
R-free | 0.25300 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.176 |
Refinement software | REFMAC (5.5.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.010 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.050 | 0.470 |
Number of reflections | 63292 | |
<I/σ(I)> | 22 | 3.5 |
Completeness [%] | 91.0 | 83 |
Redundancy | 5.7 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |