2WK8
Structure of holo form of Vibrio cholerae CqsA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 177.337, 70.134, 70.625 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.830 - 2.100 |
R-factor | 0.201 |
Rwork | 0.197 |
R-free | 0.25800 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.008 |
RMSD bond angle | 1.211 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.000 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.080 | 0.540 |
Number of reflections | 50632 | |
<I/σ(I)> | 15.3 | 2.2 |
Completeness [%] | 97.0 | 96 |
Redundancy | 5.1 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |