2WJA
Crystal structure of the tyrosine phosphatase Wzb from Escherichia coli K30 in complex with phosphate.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 90.030, 90.030, 83.540 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.500 - 2.500 |
R-factor | 0.2224 |
Rwork | 0.220 |
R-free | 0.26840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fek |
RMSD bond length | 0.002 |
RMSD bond angle | 0.570 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.080 | 0.790 |
Number of reflections | 12623 | |
<I/σ(I)> | 27.3 | 5.4 |
Completeness [%] | 90.8 | 100 |
Redundancy | 8.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2 M K2HPO4, 18% W/V PEG 3350, 0.1 M TRIS-CL PH 8.0 |