2WIP
STRUCTURE OF CDK2-CYCLIN A COMPLEXED WITH 8-ANILINO-1-METHYL-4,5-DIHYDRO- 1H-PYRAZOLO[4,3-H] QUINAZOLINE-3-CARBOXYLIC ACID
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-D |
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Collection date | 2002-04-02 |
Detector | RIGAKU R-AXIS IV |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 184.185, 184.185, 215.005 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.400 - 2.800 |
R-factor | 0.221 |
Rwork | 0.221 |
R-free | 0.25800 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.900 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS (NULL) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.080 | 0.300 |
Number of reflections | 50354 | |
<I/σ(I)> | 23.8 | 6.2 |
Completeness [%] | 94.1 | 95 |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% AMMONIUM SULPHATE, 1M KCL, 40MM HEPES PH 7 |