2WIB
Crystal Structures of the N-terminal Intracellular Domain of FeoB from Klebsiella Pneumoniae in GDP binding state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 86.552, 184.688, 38.168 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.530 - 2.560 |
R-factor | 0.222 |
Rwork | 0.222 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | STRUCTURE OF FEOB IN GMPPNP STATE |
RMSD bond length | 0.034 |
RMSD bond angle | 3.200 |
Data scaling software | CrystalClear |
Phasing software | MOLREP |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.530 | 2.650 |
High resolution limit [Å] | 2.560 | 2.560 |
Rmerge | 0.090 | 0.500 |
Number of reflections | 19651 | |
<I/σ(I)> | 23.7 | 3.9 |
Completeness [%] | 94.5 | 98.2 |
Redundancy | 6.3 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 100 MM TRIS-HCL PH 8.5, 30% PEG8000, 150 MM (NH4)2SO4 |