2WGQ
Zinc substituted E Coli Copper Amine Oxidase, a model for the precursor for 2,4,5-trihydroxyphenylalaninequinone formation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX7.2 |
Synchrotron site | SRS |
Beamline | PX7.2 |
Temperature [K] | 300 |
Detector technology | IMAGE PLATE |
Collection date | 1997-03-01 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 134.680, 166.210, 79.420 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.720 - 2.500 |
R-factor | 0.2071 |
Rwork | 0.204 |
R-free | 0.26398 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1spu |
RMSD bond length | 0.015 |
RMSD bond angle | 1.583 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0072) |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |