2WGL
Crystal structure of Helicobactor pylori UreF
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 135.163, 89.041, 65.994 |
| Unit cell angles | 90.00, 94.04, 90.00 |
Refinement procedure
| Resolution | 35.260 - 2.000 |
| R-factor | 0.1921 |
| Rwork | 0.190 |
| R-free | 0.23240 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.919 |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.120 | 2.110 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.065 | 0.241 |
| Number of reflections | 51513 | |
| <I/σ(I)> | 14.3 | 3.3 |
| Completeness [%] | 97.7 | 93.9 |
| Redundancy | 10.3 | 10 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
