2WFV
Crystal structure of DILP5 variant C4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 40.445, 40.445, 45.241 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 24.180 - 1.850 |
| R-factor | 0.202 |
| Rwork | 0.199 |
| R-free | 0.23200 |
| Structure solution method | MIR |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.389 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.180 | 1.900 |
| High resolution limit [Å] | 1.850 | 1.850 |
| Rmerge | 0.040 | 0.440 |
| Number of reflections | 3164 | |
| <I/σ(I)> | 56 | 4.54 |
| Completeness [%] | 100.0 | 99.6 |
| Redundancy | 12.8 | 10.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 20% PEG4000 |
