2WFU
Crystal structure of DILP5 variant DB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 39.789, 39.789, 45.321 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.150 - 1.850 |
R-factor | 0.219 |
Rwork | 0.215 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.465 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.150 | 1.900 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.060 | 0.170 |
Number of reflections | 3070 | |
<I/σ(I)> | 89 | 25 |
Completeness [%] | 99.7 | 100 |
Redundancy | 14.4 | 14.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% PEG4000 |