2WE7
Crystal structure of Mycobacterium tuberculosis Rv0376c homologue from Mycobacterium smegmatis
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 294 |
Detector technology | CCD |
Collection date | 2007-07-11 |
Detector | ADSC CCD |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 101.039, 101.039, 316.574 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.290 - 2.900 |
R-factor | 0.198 |
Rwork | 0.195 |
R-free | 0.25200 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.288 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.120 | 0.350 |
Number of reflections | 21926 | |
<I/σ(I)> | 63.91 | 12.1 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 26.2 | 23.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.1 M CITRATE PH 4.8, 17% PEG 8000, 0.2 M AMMONIUM ACETATE AND 4% ETHANOL BY MICRO-SEEDING |