2WDU
Fasciola hepatica sigma class GST
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS ROTATING ANODE COPPER K ALPHA |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 53.947, 87.419, 93.988 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 64.420 - 1.620 |
R-factor | 0.19262 |
Rwork | 0.191 |
R-free | 0.22384 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2w9b |
RMSD bond length | 0.014 |
RMSD bond angle | 1.428 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.700 |
High resolution limit [Å] | 1.610 | 1.610 |
Rmerge | 0.070 | 0.590 |
Number of reflections | 56342 | |
<I/σ(I)> | 16.1 | 1.7 |
Completeness [%] | 95.5 | 77.9 |
Redundancy | 4.6 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.15M KBR, 20% PEG 3350 |