2WD5

SMC hinge heterodimer (Mouse)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	CCD
Collection date	2007-04-10
Detector	ADSC CCD
Spacegroup name	P 1 21 1
Unit cell lengths	52.285, 61.867, 77.046
Unit cell angles	90.00, 105.04, 90.00

Refinement procedure

Resolution	26.050 - 2.700
R-factor	0.229
Rwork	0.225
R-free	0.30500
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.007
RMSD bond angle	1.023
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	SHARP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	26.000	2.850
High resolution limit [Å]	2.700	2.700
Rmerge	0.120	0.550
Number of reflections	10243
<I/σ(I)>	6	1.7
Completeness [%]	94.6	95.6
Redundancy	2.5	2.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1