2WBV
Canine adenovirus 2 fibre head in complex with sialic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-09-20 |
Detector | ADSC QUANTUM |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 215.000, 61.250, 143.110 |
Unit cell angles | 90.00, 131.67, 90.00 |
Refinement procedure
Resolution | 46.130 - 1.900 |
R-factor | 0.159 |
Rwork | 0.157 |
R-free | 0.19500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2j2j |
RMSD bond length | 0.008 |
RMSD bond angle | 1.266 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.100 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.150 | 0.400 |
Number of reflections | 109731 | |
<I/σ(I)> | 10.22 | 4.06 |
Completeness [%] | 99.4 | 98.8 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5% PEG 4000, 5% ISOPROPANOL, 0.1 M HEPES PH 7.4 |