2WAS
Structure of the fungal type I FAS PPT domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-06-05 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 81.120, 55.758, 81.004 |
Unit cell angles | 90.00, 111.43, 90.00 |
Refinement procedure
Resolution | 31.260 - 1.900 |
R-factor | 0.22 |
Rwork | 0.218 |
R-free | 0.25400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.077 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.600 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.070 | 0.620 |
Number of reflections | 53109 | |
<I/σ(I)> | 12 | 2.1 |
Completeness [%] | 99.6 | 90 |
Redundancy | 3.6 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | pH 4 |