2WAL
Crystal Structure of human GADD45gamma
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.2 |
| Synchrotron site | BESSY |
| Beamline | 14.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-03-12 |
| Detector | MARRESEARCH |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 108.717, 108.717, 73.371 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.810 - 2.400 |
| R-factor | 0.216 |
| Rwork | 0.215 |
| R-free | 0.25100 |
| Structure solution method | MAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.308 |
| Data reduction software | XDS |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 20.000 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.070 | |
| Number of reflections | 21647 | |
| <I/σ(I)> | 18.7 | |
| Completeness [%] | 93.0 | 80.3 |
| Redundancy | 7.09 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | 2 M MALONATE, 0.1 M BENZONATE, PH 5.5 |
