2W9P
Crystal Structure of Potato Multicystatin
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Detector | ADSC IMAGE PLATE |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 210.850, 85.710, 96.860 |
Unit cell angles | 90.00, 100.60, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.700 |
R-factor | 0.212 |
Rwork | 0.212 |
R-free | 0.24600 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.014 |
RMSD bond angle | 3.190 |
Refinement software | X-PLOR (NULL) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.700 |
Rmerge | 0.060 |
Number of reflections | 40548 |
Completeness [%] | 88.4 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |