2W8W
N100Y SPT with PLP-ser
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 73.600, 107.130, 89.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.480 - 2.140 |
R-factor | 0.195 |
Rwork | 0.192 |
R-free | 0.24900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.090 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | REFMAC (5.5.0070) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.000 | 2.200 |
High resolution limit [Å] | 2.140 | 2.140 |
Rmerge | 0.060 | 0.470 |
Number of reflections | 19876 | |
<I/σ(I)> | 17.8 | 2.9 |
Completeness [%] | 99.5 | 97 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |