2W8V
SPT with PLP, N100W
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 71.920, 109.786, 91.774 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.450 - 1.430 |
R-factor | 0.162 |
Rwork | 0.161 |
R-free | 0.18900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.208 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | REFMAC (5.5.0070) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.000 | 1.470 |
High resolution limit [Å] | 1.430 | 1.430 |
Rmerge | 0.040 | 0.390 |
Number of reflections | 62574 | |
<I/σ(I)> | 21 | 3.1 |
Completeness [%] | 98.0 | 88 |
Redundancy | 4.7 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |