2W8I
Crystal structure of Wza24-345.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 140.084, 140.202, 165.226 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.380 - 3.000 |
R-factor | 0.211 |
Rwork | 0.210 |
R-free | 0.23100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2j58 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.093 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.120 | 0.900 |
Number of reflections | 65664 | |
<I/σ(I)> | 13.8 | 1.8 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 5.6 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M HEPES PH 7.1, 0.2 M CACL2, 19% PEG 400. |