2W6J
Low resolution structures of bovine mitochondrial F1-ATPase during controlled dehydration: Hydration State 5.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 294 |
Detector technology | CCD |
Collection date | 2008-09-17 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 106.930, 124.070, 264.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 132.450 - 3.840 |
R-factor | 0.305 |
Rwork | 0.305 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bmf |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0038) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.800 | 4.050 |
High resolution limit [Å] | 3.840 | 3.840 |
Rmerge | 0.150 | 0.260 |
Number of reflections | 32818 | |
<I/σ(I)> | 11.5 | 2.7 |
Completeness [%] | 96.1 | 92.8 |
Redundancy | 2.5 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 50 MM TRIS-HCL PH 8.2, 200 MM NACL, 20 MM MGSO4, 1 MM ADP, 1 MM ALCL3, 6 MM NAF 0.004% (W/V)PHENYLMETHYLSULFONYL FLUORIDE AND 12% (W/V) POLYETHYLENE GLYCOL 6000 |