2W61
Saccharomyces cerevisiae Gas2p apostructure (E176Q mutant)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.883, 64.479, 152.038 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.620 |
R-factor | 0.176 |
Rwork | 0.175 |
R-free | 0.21700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | DERIVATIVE MODEL NOT DEPOSITED |
RMSD bond length | 0.012 |
RMSD bond angle | 1.278 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.680 |
High resolution limit [Å] | 1.620 | 1.620 |
Rmerge | 0.050 | 0.250 |
Number of reflections | 64209 | |
<I/σ(I)> | 18.4 | 4.12 |
Completeness [%] | 98.2 | 96.6 |
Redundancy | 3.6 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 100 MM SODIUM ACETATE PH 4.5; 5% ACETONE; 20% 1,4-BUTANEDIOL |