2W5L
RNASE A-NADP COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-01-17 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 102.890, 33.699, 74.252 |
Unit cell angles | 90.00, 89.97, 90.00 |
Refinement procedure
Resolution | 74.330 - 1.700 |
R-factor | 0.185 |
Rwork | 0.183 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1afu |
RMSD bond length | 0.015 |
RMSD bond angle | 1.386 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.4.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.040 | 0.100 |
Number of reflections | 27006 | |
<I/σ(I)> | 21.3 | 10.3 |
Completeness [%] | 94.8 | 88.3 |
Redundancy | 5.79 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 20% PEG 4000, 0.02M SODIUM CITRATE BUFFER, PH 5.5 |