2W5I
RNASE A-AP3A COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2001-08-03 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 101.960, 33.402, 75.703 |
Unit cell angles | 90.00, 91.05, 90.00 |
Refinement procedure
Resolution | 75.590 - 2.400 |
R-factor | 0.198 |
Rwork | 0.190 |
R-free | 0.27300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1afu |
RMSD bond length | 0.014 |
RMSD bond angle | 1.608 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.4.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.090 | 0.340 |
Number of reflections | 9496 | |
<I/σ(I)> | 10.8 | 2 |
Completeness [%] | 92.3 | 94.6 |
Redundancy | 2.39 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 20% PEG 4000, 0.02M SODIUM CITRATE BUFFER, PH 5.5 |