2W46
CBM35 from Cellvibrio japonicus Abf62
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 80 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 1 |
Unit cell lengths | 28.216, 46.135, 49.006 |
Unit cell angles | 71.61, 89.78, 82.19 |
Refinement procedure
Resolution | 23.880 - 1.900 |
R-factor | 0.141 |
Rwork | 0.137 |
R-free | 0.21800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.562 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.900 | 1.950 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.120 | 0.290 |
Number of reflections | 16341 | |
<I/σ(I)> | 10.6 | 2.4 |
Completeness [%] | 94.1 | 90.8 |
Redundancy | 1.7 | 1.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.9 | 0.4M SODIUM THIOCYANATE, 20% PEG3350, pH 6.9 |