2W3J
Structure of a family 35 carbohydrate binding module from an environmental isolate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | H 3 |
Unit cell lengths | 83.943, 83.943, 79.498 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 53.680 - 1.700 |
R-factor | 0.163 |
Rwork | 0.162 |
R-free | 0.18800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.367 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.000 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.070 | 0.480 |
Number of reflections | 22914 | |
<I/σ(I)> | 15.7 | 2.5 |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 5.3 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.2 | 20% POLYETHYLENE GLYCOL 8000, 0.2M NACL, 0.25M NA CITRATE PH 4.2, 0.25M NA DIHYDROGEN PHOSPHATE PH 4.2 |