2W2U
STRUCTURAL INSIGHT INTO THE INTERACTION BETWEEN ARCHAEAL ESCRT-III AND AAA-ATPASE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-23 |
Detector | MARRESEARCH |
Spacegroup name | P 43 |
Unit cell lengths | 49.855, 49.855, 107.672 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.880 - 2.200 |
R-factor | 0.227 |
Rwork | 0.225 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v6y |
RMSD bond length | 0.008 |
RMSD bond angle | 1.043 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.880 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.140 | 0.520 |
Number of reflections | 12626 | |
<I/σ(I)> | 16.2 | 3.7 |
Completeness [%] | 99.5 | 99.5 |
Redundancy | 7.2 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 15% PEG4K, 0.1M TRIS(PH7.5) |