2W24
M. tuberculosis Rv3291c complexed to Lysine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 100.980, 100.980, 99.311 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.430 - 2.500 |
R-factor | 0.193 |
Rwork | 0.191 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ivm |
RMSD bond length | 0.026 |
RMSD bond angle | 2.540 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.430 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.090 | 0.630 |
Number of reflections | 18364 | |
<I/σ(I)> | 5.29 | 2.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.5 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6.0 |