2W0L
CRYSTAL STRUCTURE OF THE MUTANT H8P FROM THE RECOMBINANT VARIABLE DOMAIN 6JAL2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-24 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.940, 85.495, 69.152 |
Unit cell angles | 90.00, 91.20, 90.00 |
Refinement procedure
Resolution | 35.560 - 2.200 |
R-factor | 0.208 |
Rwork | 0.206 |
R-free | 0.24500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2cd0 |
RMSD bond length | 0.020 |
RMSD bond angle | 2.054 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.700 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.040 | 0.100 |
Number of reflections | 22584 | |
<I/σ(I)> | 16.1 | 6.6 |
Completeness [%] | 78.8 | 43.9 |
Redundancy | 1.6 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |